Abstract

‘‘Amorphous’’ Ni60Nb40 has been prepared by mechanical alloying of elemental nickel and niobium powders in a laboratory ball mill in controlled environments. X-ray diffraction was used to follow the progress of the mechanical alloying which eventually produced ‘‘amorphous’’ diffraction patterns similar to those for liquid quenched amorphous Ni60Nb40. Crystallization behavior was measured by differential scanning calorimetry for the mechanically alloyed and liquid quenched material. The differences that were observed in this behavior, and in the products of crystallization, may be attributed to impurities (especially oxygen) introduced during mechanical alloying.

Keywords

Materials scienceDifferential scanning calorimetryAmorphous solidCrystallizationImpurityNiobiumBall millMetallurgyAmorphous metalDiffractionChemical engineeringCrystallographyAlloyChemistryThermodynamicsOrganic chemistry

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Publication Info

Year
1983
Type
article
Volume
43
Issue
11
Pages
1017-1019
Citations
1092
Access
Closed

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C.C. Koch, O.B. Cavin, C.G. McKamey et al. (1983). Preparation of ‘‘amorphous’’ Ni60Nb40 by mechanical alloying. Applied Physics Letters , 43 (11) , 1017-1019. https://doi.org/10.1063/1.94213

Identifiers

DOI
10.1063/1.94213