Abstract
..cap alpha..-Sulfur, S/sub 8/, M/sub r/=256.51, orthorhombic, Fddd, a=10.4646(1), b=12.8660(1), c=24.4860(3) A, V=3296.7 A/sup 3/, Z=16, D/sub x/=2.067 g cm/sup -3/, Mo K..cap alpha.., lambda..cap alpha../sub 1/=0.70930 A, ..mu..=19.90 cm/sup -1/, F(000)=2048, T=298 K, R=0.019, wR=0.023 for 851 reflections with Igreater than or equal to3sigma(I), R=0.019 (wR=0.020) for 506 reflections with Igreater than or equal to3sigma(I) and (sintheta)/lambdagreater than or equal to0.481 A/sup -1/. Mean structural parameters are the same for both refinements: S-S=2.046(3) (uncorrected) and 2.055(2) A (corrected for libration), S-S-S=108.2(6) and S-S-S-S=98.5(19)/sup 0/.
Keywords
Orthorhombic crystal systemCrystallographySulfurX-ray crystallographyLambdaPhysicsCrystal structureChemistryMaterials scienceDiffractionMetallurgyOptics
Related Publications
The diffraction of X-rays by distorted-crystal aggregates. II. Diffraction by bent lamellae
The apparent particle size of distorted crystallites varies from independence of θ and λ (particle-size broadening) to proportionality with λ cosec θ (distortion broadening) as ...
Synthesis, structure, and photovoltaic property of a nanocrystalline 2H perovskite-type novel sensitizer (CH3CH2NH3)PbI3
Abstract A new nanocrystalline sensitizer with the chemical formula (CH 3 CH 2 NH 3 )PbI 3 is synthesized by reacting ethylammonium iodide with lead iodide, and its crystal stru...
Publication Info
- Year
- 1987
- Type
- article
- Volume
- 43
- Issue
- 12
- Pages
- 2260-2262
- Citations
- 174
- Access
- Closed
External Links
Social Impact
Altmetric
PlumX Metrics
Social media, news, blog, policy document mentions
Citation Metrics
174
OpenAlex
Cite This
S. J. Rettig,
J. Trotter
(1987).
Refinement of the structure of orthorhombic sulfur, α-S8.
Acta Crystallographica Section C Crystal Structure Communications
, 43
(12)
, 2260-2262.
https://doi.org/10.1107/s0108270187088152
Identifiers
- DOI
- 10.1107/s0108270187088152